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有色金屬冶金學實驗教程（簡體書）
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本書是依據有色金屬冶金學課程內容而設計匯總了相應的系列教學實驗編寫而成的，實驗主要由有色冶金中的火法實驗、濕法實驗及電冶金實驗三部分共十八個教學實驗組成。其中有以教學演示為主的示範性實驗，有以學生自主動手操作的啟發性實驗，使學生在學習掌握了有色金屬冶金學課程教學理論內容基礎上，通過開展教學實驗操作加深對有色金屬冶煉原理和工藝過程知識的理解和運用，使冶金工程專業的本科生瞭解試驗研究工作的程序，掌握試驗方法和技能，培養學生分析和解決冶金工程實際問題的能力。本書為冶金工程專業教材，可為師生提供實驗教學依據和指導，也可供相關專業的企業工程技術或科研人員參考。
目次
目錄實驗一白雲石煆燒實驗.................................................................................................................................11.1實驗目的................................................................................................................................................
11.2實驗原理................................................................................................................................................11.3實驗儀器與試劑..................................................................................................................................
21.4實驗步驟................................................................................................................................................21.5注意事項................................................................................................................................................
21.6實驗記錄................................................................................................................................................21.7實驗數據處理與報告編寫...............................................................................................................
31.8思考題.....................................................................................................................................................3實驗二熱失重法測定炭陽極的氧化速率................................................................................................
52.1實驗目的.................................................................................................................................................52.2實驗原理................................................................................................................................................
52.3實驗儀器與裝置..................................................................................................................................62.4實驗步驟................................................................................................................................................
72.5注意事項................................................................................................................................................82.6實驗記錄................................................................................................................................................
82.7實驗數據處理與報告編寫...............................................................................................................82.8思考題.....................................................................................................................................................
9實驗三矽熱法煉鎂實驗..............................................................................................................................103.1實驗目的...............................................................................................................................................
103.2實驗原理.............................................................................................................................................103.3實驗儀器與試劑...............................................................................................................................
113.4實驗步驟.............................................................................................................................................123.5注意事項.............................................................................................................................................
133.6實驗記錄.............................................................................................................................................133.7實驗數據處理與報告編寫.............................................................................................................
143.8思考題..................................................................................................................................................14實驗四鉛錫合金的真空蒸餾分離..............................................................................................................
164.1實驗目的.............................................................................................................................................164.2實驗原理.............................................................................................................................................
164.3實驗儀器與試劑...............................................................................................................................184.4實驗步驟.............................................................................................................................................
194.5注意事項.............................................................................................................................................204.6實驗記錄.............................................................................................................................................
204.7實驗數據處理與報告編寫.............................................................................................................204.8思考題..................................................................................................................................................
21實驗五熔鹽電解質初晶溫度的測定實驗..............................................................................................225.1實驗目的.............................................................................................................................................
225.2實驗原理.............................................................................................................................................225.3實驗儀器與試劑...............................................................................................................................
225.4實驗步驟.............................................................................................................................................235.5注意事項.............................................................................................................................................
245.6實驗記錄.............................................................................................................................................245.7實驗數據處理與報告編寫.............................................................................................................
245.8思考題..................................................................................................................................................25實驗六熔鹽電解質密度的測定實驗.........................................................................................................
266.1實驗目的.............................................................................................................................................266.2實驗原理.............................................................................................................................................
266.3實驗裝置和材料...............................................................................................................................276.4實驗步驟.............................................................................................................................................
286.5注意事項.............................................................................................................................................306.6實驗數據處理....................................................................................................................................
306.7思考題..................................................................................................................................................30實驗七熔鹽電解質電導率的測定實驗..................................................................................................
317.1實驗目的...............................................................................................................................................317.2實驗原理.............................................................................................................................................
317.3實驗裝置和材料...............................................................................................................................337.4實驗步驟.............................................................................................................................................
347.5注意事項.............................................................................................................................................367.6實驗數據處理....................................................................................................................................
367.7思考題..................................................................................................................................................36實驗八方鉛礦的三氯化鐵浸出實驗.......................................................................................................
378.1實驗目的.............................................................................................................................................378.2實驗原理.............................................................................................................................................
378.3實驗儀器與試劑...............................................................................................................................388.4實驗步驟.............................................................................................................................................
388.5注意事項.............................................................................................................................................398.6實驗記錄.............................................................................................................................................
398.7實驗數據處理與報告編寫.............................................................................................................408.8思考題..................................................................................................................................................
40實驗九鋅焙砂的浸出過程實驗...................................................................................................................419.1實驗目的...............................................................................................................................................
419.2原理.......................................................................................................................................................419.3設備及實驗裝置.................................................................................................................................
429.4實驗步驟.............................................................................................................................................439.5實驗記錄.............................................................................................................................................
449.6數據處理和報告編寫......................................................................................................................449.7思考題...................................................................................................................................................
44實驗十鋁土礦的高壓溶出實驗................................................................................................................4510.1實驗目的...........................................................................................................................................
4510.2實驗原理...........................................................................................................................................4510.3實驗儀器與試劑.............................................................................................................................
4710.4實驗步驟...........................................................................................................................................4710.5注意事項...........................................................................................................................................
4810.6實驗記錄...........................................................................................................................................4910.7實驗數據處理與報告編寫..........................................................................................................
5010.8思考題................................................................................................................................................50實驗十一N235萃取分離鎳和鈷實驗.......................................................................................................
5111.1實驗目的...........................................................................................................................................5111.2實驗原理...........................................................................................................................................
5111.3實驗儀器與試劑.............................................................................................................................5311.4實驗步驟...........................................................................................................................................
5311.5注意事項...........................................................................................................................................5411.6實驗記錄...........................................................................................................................................
5411.7實驗數據處理與報告編寫...........................................................................................................5511.8思考題................................................................................................................................................
56實驗十二電導率法測定底吹煉銅爐水模型的混勻時間實驗........................................................5712.1實驗目的...........................................................................................................................................5712.2實驗原理...........................................................................................................................................
5712.3實驗儀器及試劑.............................................................................................................................5912.4實驗步驟...........................................................................................................................................
6012.5注意事項...........................................................................................................................................6212.6實驗記錄...........................................................................................................................................
6212.7實驗數據處理與報告編寫..........................................................................................................6212.8思考題................................................................................................................................................
63實驗十三鎂電解過程反電動勢的測量實驗...........................................................................................6413.1實驗目的...........................................................................................................................................
6413.2實驗原理...........................................................................................................................................6413.3實驗儀器與試劑.............................................................................................................................
6613.4實驗步驟...........................................................................................................................................6713.5注意事項...........................................................................................................................................
6813.6實驗記錄...........................................................................................................................................6813.7實驗數據處理與報告編寫..........................................................................................................
6813.8思考題................................................................................................................................................68實驗十四鋁電解過程中臨界電流密度的測定.......................................................................................
6914.1實驗目的...........................................................................................................................................6914.2原理......................................................................................................................................................
6914.3設備及實驗裝置.............................................................................................................................7114.4實驗步驟............................................................................................................................................
7214.5注意事項............................................................................................................................................7314.6實驗記錄...........................................................................................................................................
7314.7編寫報告............................................................................................................................................7314.8思考題................................................................................................................................................
74實驗十五硫酸鋅溶液的電解沉積實驗..................................................................................................7515.1實驗目的...........................................................................................................................................
7515.2實驗原理...........................................................................................................................................7515.3實驗儀器與試劑.............................................................................................................................
7615.4實驗步驟...........................................................................................................................................7715.5注意事項...........................................................................................................................................
7915.6實驗記錄...........................................................................................................................................7915.7實驗數據處理與報告編寫..........................................................................................................
8015.8思考題................................................................................................................................................80實驗十六電位掃描法測鎳陽極極化曲線實驗....................................................................................
8116.1實驗目的...........................................................................................................................................8116.2實驗原理...........................................................................................................................................
8116.3實驗儀器與試劑.............................................................................................................................8216.4實驗步驟...........................................................................................................................................
8316.5注意事項...........................................................................................................................................8316.6實驗記錄...........................................................................................................................................
8416.7實驗數據處理與報告編寫..........................................................................................................8416.8思考題................................................................................................................................................
84實驗十七銅的電解精煉實驗.......................................................................................................................8517.1實驗目的...........................................................................................................................................
8517.2實驗基本原理..................................................................................................................................8517.3實驗原料及設備.............................................................................................................................
8617.4實驗步驟和現象.............................................................................................................................8717.5實驗結果及數據處理.....................................................................................................................
8717.6實驗討論...........................................................................................................................................8817.7思考題................................................................................................................................................
88實驗十八金屬及合金的微弧氧化實驗..................................................................................................8918.1實驗目的...........................................................................................................................................
8918.2實驗原理...........................................................................................................................................8918.3實驗儀器與試劑.............................................................................................................................
8918.4實驗步驟...........................................................................................................................................9018.5注意事項...........................................................................................................................................
9118.6實驗記錄...........................................................................................................................................9118.7實驗數據處理與報告編寫..........................................................................................................
9218.8思考題................................................................................................................................................92附錄實驗誤差與數據處理..........................................................................................................................
931實驗誤差.................................................................................................................................................931.1一些有關的基本概念......................................................................................................................
931.2誤差的分類.........................................................................................................................................941.3偶然誤差的正態分佈......................................................................................................................
951.4標准偏差與誤差函數......................................................................................................................961.5算術平均值與殘差...........................................................................................................................
971.6測量結果的置信度...........................................................................................................................981.7可疑數據的剔除...............................................................................................................................
981.8絕對誤差與相對誤差......................................................................................................................992有效數字和計算規則..........................................................................................................................
993間接測量中的誤差............................................................................................................................1014實驗數據處理方法............................................................................................................................
1034.1列表法...............................................................................................................................................1034.2圖解法...............................................................................................................................................
1044.3逐差法...............................................................................................................................................1064.4最小二乘法......................................................................................................................................
107參考文獻............................................................................................................................................................110
11.2實驗原理................................................................................................................................................11.3實驗儀器與試劑..................................................................................................................................
21.4實驗步驟................................................................................................................................................21.5注意事項................................................................................................................................................
21.6實驗記錄................................................................................................................................................21.7實驗數據處理與報告編寫...............................................................................................................
31.8思考題.....................................................................................................................................................3實驗二熱失重法測定炭陽極的氧化速率................................................................................................
52.1實驗目的.................................................................................................................................................52.2實驗原理................................................................................................................................................
52.3實驗儀器與裝置..................................................................................................................................62.4實驗步驟................................................................................................................................................
72.5注意事項................................................................................................................................................82.6實驗記錄................................................................................................................................................
82.7實驗數據處理與報告編寫...............................................................................................................82.8思考題.....................................................................................................................................................
9實驗三矽熱法煉鎂實驗..............................................................................................................................103.1實驗目的...............................................................................................................................................
103.2實驗原理.............................................................................................................................................103.3實驗儀器與試劑...............................................................................................................................
113.4實驗步驟.............................................................................................................................................123.5注意事項.............................................................................................................................................
133.6實驗記錄.............................................................................................................................................133.7實驗數據處理與報告編寫.............................................................................................................
143.8思考題..................................................................................................................................................14實驗四鉛錫合金的真空蒸餾分離..............................................................................................................
164.1實驗目的.............................................................................................................................................164.2實驗原理.............................................................................................................................................
164.3實驗儀器與試劑...............................................................................................................................184.4實驗步驟.............................................................................................................................................
194.5注意事項.............................................................................................................................................204.6實驗記錄.............................................................................................................................................
204.7實驗數據處理與報告編寫.............................................................................................................204.8思考題..................................................................................................................................................
21實驗五熔鹽電解質初晶溫度的測定實驗..............................................................................................225.1實驗目的.............................................................................................................................................
225.2實驗原理.............................................................................................................................................225.3實驗儀器與試劑...............................................................................................................................
225.4實驗步驟.............................................................................................................................................235.5注意事項.............................................................................................................................................
245.6實驗記錄.............................................................................................................................................245.7實驗數據處理與報告編寫.............................................................................................................
245.8思考題..................................................................................................................................................25實驗六熔鹽電解質密度的測定實驗.........................................................................................................
266.1實驗目的.............................................................................................................................................266.2實驗原理.............................................................................................................................................
266.3實驗裝置和材料...............................................................................................................................276.4實驗步驟.............................................................................................................................................
286.5注意事項.............................................................................................................................................306.6實驗數據處理....................................................................................................................................
306.7思考題..................................................................................................................................................30實驗七熔鹽電解質電導率的測定實驗..................................................................................................
317.1實驗目的...............................................................................................................................................317.2實驗原理.............................................................................................................................................
317.3實驗裝置和材料...............................................................................................................................337.4實驗步驟.............................................................................................................................................
347.5注意事項.............................................................................................................................................367.6實驗數據處理....................................................................................................................................
367.7思考題..................................................................................................................................................36實驗八方鉛礦的三氯化鐵浸出實驗.......................................................................................................
378.1實驗目的.............................................................................................................................................378.2實驗原理.............................................................................................................................................
378.3實驗儀器與試劑...............................................................................................................................388.4實驗步驟.............................................................................................................................................
388.5注意事項.............................................................................................................................................398.6實驗記錄.............................................................................................................................................
398.7實驗數據處理與報告編寫.............................................................................................................408.8思考題..................................................................................................................................................
40實驗九鋅焙砂的浸出過程實驗...................................................................................................................419.1實驗目的...............................................................................................................................................
419.2原理.......................................................................................................................................................419.3設備及實驗裝置.................................................................................................................................
429.4實驗步驟.............................................................................................................................................439.5實驗記錄.............................................................................................................................................
449.6數據處理和報告編寫......................................................................................................................449.7思考題...................................................................................................................................................
44實驗十鋁土礦的高壓溶出實驗................................................................................................................4510.1實驗目的...........................................................................................................................................
4510.2實驗原理...........................................................................................................................................4510.3實驗儀器與試劑.............................................................................................................................
4710.4實驗步驟...........................................................................................................................................4710.5注意事項...........................................................................................................................................
4810.6實驗記錄...........................................................................................................................................4910.7實驗數據處理與報告編寫..........................................................................................................
5010.8思考題................................................................................................................................................50實驗十一N235萃取分離鎳和鈷實驗.......................................................................................................
5111.1實驗目的...........................................................................................................................................5111.2實驗原理...........................................................................................................................................
5111.3實驗儀器與試劑.............................................................................................................................5311.4實驗步驟...........................................................................................................................................
5311.5注意事項...........................................................................................................................................5411.6實驗記錄...........................................................................................................................................
5411.7實驗數據處理與報告編寫...........................................................................................................5511.8思考題................................................................................................................................................
56實驗十二電導率法測定底吹煉銅爐水模型的混勻時間實驗........................................................5712.1實驗目的...........................................................................................................................................5712.2實驗原理...........................................................................................................................................
5712.3實驗儀器及試劑.............................................................................................................................5912.4實驗步驟...........................................................................................................................................
6012.5注意事項...........................................................................................................................................6212.6實驗記錄...........................................................................................................................................
6212.7實驗數據處理與報告編寫..........................................................................................................6212.8思考題................................................................................................................................................
63實驗十三鎂電解過程反電動勢的測量實驗...........................................................................................6413.1實驗目的...........................................................................................................................................
6413.2實驗原理...........................................................................................................................................6413.3實驗儀器與試劑.............................................................................................................................
6613.4實驗步驟...........................................................................................................................................6713.5注意事項...........................................................................................................................................
6813.6實驗記錄...........................................................................................................................................6813.7實驗數據處理與報告編寫..........................................................................................................
6813.8思考題................................................................................................................................................68實驗十四鋁電解過程中臨界電流密度的測定.......................................................................................
6914.1實驗目的...........................................................................................................................................6914.2原理......................................................................................................................................................
6914.3設備及實驗裝置.............................................................................................................................7114.4實驗步驟............................................................................................................................................
7214.5注意事項............................................................................................................................................7314.6實驗記錄...........................................................................................................................................
7314.7編寫報告............................................................................................................................................7314.8思考題................................................................................................................................................
74實驗十五硫酸鋅溶液的電解沉積實驗..................................................................................................7515.1實驗目的...........................................................................................................................................
7515.2實驗原理...........................................................................................................................................7515.3實驗儀器與試劑.............................................................................................................................
7615.4實驗步驟...........................................................................................................................................7715.5注意事項...........................................................................................................................................
7915.6實驗記錄...........................................................................................................................................7915.7實驗數據處理與報告編寫..........................................................................................................
8015.8思考題................................................................................................................................................80實驗十六電位掃描法測鎳陽極極化曲線實驗....................................................................................
8116.1實驗目的...........................................................................................................................................8116.2實驗原理...........................................................................................................................................
8116.3實驗儀器與試劑.............................................................................................................................8216.4實驗步驟...........................................................................................................................................
8316.5注意事項...........................................................................................................................................8316.6實驗記錄...........................................................................................................................................
8416.7實驗數據處理與報告編寫..........................................................................................................8416.8思考題................................................................................................................................................
84實驗十七銅的電解精煉實驗.......................................................................................................................8517.1實驗目的...........................................................................................................................................
8517.2實驗基本原理..................................................................................................................................8517.3實驗原料及設備.............................................................................................................................
8617.4實驗步驟和現象.............................................................................................................................8717.5實驗結果及數據處理.....................................................................................................................
8717.6實驗討論...........................................................................................................................................8817.7思考題................................................................................................................................................
88實驗十八金屬及合金的微弧氧化實驗..................................................................................................8918.1實驗目的...........................................................................................................................................
8918.2實驗原理...........................................................................................................................................8918.3實驗儀器與試劑.............................................................................................................................
8918.4實驗步驟...........................................................................................................................................9018.5注意事項...........................................................................................................................................
9118.6實驗記錄...........................................................................................................................................9118.7實驗數據處理與報告編寫..........................................................................................................
9218.8思考題................................................................................................................................................92附錄實驗誤差與數據處理..........................................................................................................................
931實驗誤差.................................................................................................................................................931.1一些有關的基本概念......................................................................................................................
931.2誤差的分類.........................................................................................................................................941.3偶然誤差的正態分佈......................................................................................................................
951.4標准偏差與誤差函數......................................................................................................................961.5算術平均值與殘差...........................................................................................................................
971.6測量結果的置信度...........................................................................................................................981.7可疑數據的剔除...............................................................................................................................
981.8絕對誤差與相對誤差......................................................................................................................992有效數字和計算規則..........................................................................................................................
993間接測量中的誤差............................................................................................................................1014實驗數據處理方法............................................................................................................................
1034.1列表法...............................................................................................................................................1034.2圖解法...............................................................................................................................................
1044.3逐差法...............................................................................................................................................1064.4最小二乘法......................................................................................................................................
107參考文獻............................................................................................................................................................110
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特別提醒：部分書籍附贈之內容(如音頻mp3或影片dvd等)已無實體光碟提供，需以QR CODE 連結至當地網站註冊“並通過驗證程序”，方可下載使用。
無現貨庫存之簡體書，將向海外調貨：
海外有庫存之書籍，等候約45個工作天;
海外無庫存之書籍，平均作業時間約60個工作天，然不保證確定可調到貨，尚請見諒。
為了保護您的權益，「三民網路書店」提供會員七日商品鑑賞期(收到商品為起始日)。
若要辦理退貨，請在商品鑑賞期內寄回，且商品必須是全新狀態與完整包裝(商品、附件、發票、隨貨贈品等)否則恕不接受退貨。